Category Archives: MyResearch

Alleviating industrial uncertainty

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Want to know how to assess the quality of predictions of structural deformation from a computational model and how to diagnose the causes of differences between measurements and predictions?  The MOTIVATE project has the answers; that might seem like an over-assertive claim but read on and make your own judgment.  Eighteen months ago, I reported on a new method for quantifying the uncertainty present in measurements of deformation made in an industrial environment [see ‘Industrial uncertainty’ on December 12th, 2018] that we were trialling on a 1 m square panel of an aircraft fuselage.  Recently, we have used the measurement uncertainty we found to make judgments about the quality of predictions from computer models of the panel under compressive loading.  The top graphic shows the outside surface of the panel (left) with a speckle pattern to allow measurements of its deformation using digital image correlation (DIC) [see ‘256 shades of grey‘ on January 22, 2014 for a brief explanation of DIC]; and the inside surface (right) with stringers and ribs.  The bottom graphic shows our results for two load cases: a 50 kN compression (top row) and a 50 kN compression and 1 degree of torsion (bottom row).  The left column shows the out-of-plane deformation measured using a stereoscopic DIC system and the middle row shows the corresponding predictions from a computational model using finite element analysis [see ‘Did cubism inspire engineering analysis?’ on January 25th, 2017].  We have described these deformation fields in a reduced form using feature vectors by applying image decomposition [see ‘Recognizing strain’ on October 28th, 2015 for a brief explanation of image decomposition].  The elements of the feature vectors are known as shape descriptors and corresponding pairs of them, from the measurements and predictions, are plotted in the graphs on the right in the bottom graphic for each load case.  If the predictions were in perfect agreement with measurements then all of the points on these graphs would lie on the line equality [y=x] which is the solid line on each graph.  However, perfect agreement is unobtainable because there will always be uncertainty present; so, the question arises, how much deviation from the solid line is acceptable?  One answer is that the deviation should be less than the uncertainty present in the measurements that we evaluated with our new method and is shown by the dashed lines.  Hence, when all of the points fall inside the dashed lines then the predictions are at least as good as the measurements.  If some points lie outside of the dashed lines, then we can look at the form of the corresponding shape descriptors to start diagnosing why we have significant differences between our model and experiment.  The forms of these outlying shape descriptors are shown as insets on the plots.  However, busy, or non-technical decision-makers are often not interested in this level of detailed analysis and instead just want to know how good the predictions are.  To answer this question, we have implemented a validation metric (VM) that we developed [see ‘Million to one’ on November 21st, 2018] which allows us to state the probability that the predictions and measurements are from the same population given the known uncertainty in the measurements – these probabilities are shown in the black boxes superimposed on the graphs.

These novel methods create a toolbox for alleviating uncertainty about predictions of structural behaviour in industrial contexts.  Please get in touch if you want more information in order to test these tools yourself.

The MOTIVATE project has received funding from the Clean Sky 2 Joint Undertaking under the European Union’s Horizon 2020 research and innovation programme under grant agreement No. 754660 and the Swiss State Secretariat for Education, Research and Innovation under contract number 17.00064.

The opinions expressed in this blog post reflect only the author’s view and the Clean Sky 2 Joint Undertaking is not responsible for any use that may be made of the information it contains.

Spatio-temporal damage maps for composite materials

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Earlier this year, my group published a new technique for illustrating the development of damage as a function of both space and time in materials during testing in a laboratory.  The information is presented in a damage-time map and shows where and when damage appears in the material.  The maps are based on the concept that damage represents a change in the structure of the material and, hence, produces changes in the load paths or stress distribution in the material.  We can use any of a number of optical techniques to measure strain, which is directly related to stress, across the surface of the material; and then look for changes in the strain distribution in real-time.  Wherever a permanent change is seen to occur there must also be permanent deformation or damage. We use image decomposition techniques that we developed some time ago [see ‘Recognizing strain‘ on October 28th, 2018], to identify the changes. Our damage-time maps remove the need for skilled operators to spend large amounts of time reviewing data and making subjective decisions.  They also allow a large amount of information to be presented in a single image which makes detailed comparisons with computer predictions easier and more readily quantifiable that, in turn, supports the validation of computational models [see ‘Model validation‘ on September 18th, 2012].

The structural integrity of composite materials is an on-going area of research because we only have a limited understanding of these materials.  It is easy to design structures using materials that have a uniform or homogeneous structure and mechanical properties which do not vary with orientation, i.e. isotropic properties.  For simple components, an engineer can predict the stresses and likely failure modes using the laws of physics, a pencil and paper plus perhaps a calculator.  However, when materials contain fibres embedded in a matrix, such as carbon-fibres in an epoxy resin, then the analysis of structural behaviour becomes much more difficult due to the interaction between the fibres and with the matrix.  Of course, these interactions are also what make these composite materials interesting because they allow less material to be used to achieve the same performance as homogeneous isotropic materials.  There are very many ways of arranging fibres in a matrix as well as many different types of fibres and matrix; and, engineers do not understand most of their interactions nor the mechanisms that lead to failure.

The image shows, on the left, the maximum principal strain in a composite specimen loaded longitudinally in tension to just before failure; and, on the right, the corresponding damage-time map indicating when and where damage developing during the tension loading.

Source:

Christian WJR, Dvurecenska K, Amjad K, Pierce J, Przybyla C & Patterson EA, Real-time quantification of damage in structural materials during mechanical testing, Royal Society Open Science, 7:191407, 2020.

Salt increases nanoparticle diffusion

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About two and half years ago, I wrote about an article we had published on the motion of nanoparticles [see ‘Slow moving nanoparticles‘ on December 13th, 2017] in which we had shown that, for very small particles at low concentrations, the motion of a particle is independent of its size and does not flow the well-known Stokes-Einstein law.  Our article presented convincing evidence from experiments to support our conclusions but was light on explanation in terms of the mechanics.  At the end of last year, we published a short article in Scientific Reports, in which we demonstrated that the motion of nanoparticles at low concentrations is dependent on the interaction of van der Waals forces and electrostatic forces.  Van der Waals forces are short-range attractive forces between uncharged molecules due to interacting dipole moments, whereas the electrostatic forces are the repulsion of electric charges.  We changed both of these forces by using salt solutions of different concentration and observing the changes in nanoparticle behaviour.  Increasing the molarity increases the diffusion of the particles until the solution is saturated, as shown in the picture for 50 nanometre diameter gold particles (that’s about half the diameter of a coronavirus particle or one thousandth of the diameter of a human hair).  Our findings have implications for understanding the behaviour of nanoparticles dispersed in biological media, which typically contain salt in solution, because the concentration of salt ions in the medium affects nanoparticle diffusion that has been shown to influence cellular uptake and toxicity.

Sources:

Coglitore D, Edwardson SP, Macko P, Patterson EA, Whelan MP, Transition from fractional to classical Stokes-Einstein behaviour in simple fluids, Royal Society Open Science, 4:170507, 2017.

Giorgi F, Coglitore D, Curran JM, Gilliland D, Macko P, Whelan M, Worth A & Patterson EA, The influence of inter-particle forces on diffusion at the nanoscale, Scientific Reports, 9:12689, 2019.

Try the impossible to achieve the unusual

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Everyone who attends a certain type of English school is given a nickname.  Mine was Floyd Patterson. In 1956, Floyd Patterson was the youngest boxer to become the world heavyweight champion.  I was certainly not a heavyweight but perhaps I was pugnacious in defending myself against larger and older boys.  Floyd Patterson had a maxim that drove his career: ‘you try the impossible to achieve the unusual’.  I have used this approach in various leadership roles and in guiding my research students for many years by encouraging them to throw away caution in planning their PhD programmes.   I only made the connection with Floyd Patterson recently when reading Edward O. Wilson‘s book, ‘Letters to a Young Scientist‘.  Previously, I had associated it with Edmund Hillary’s biography that is titled ‘Nothing Venture, Nothing Win’, which is peculiar corruption of a quote, often attributed to Benjamin Franklin but that probably originated much earlier, ‘Nothing ventured, nothing gained’.  I read Hillary’s book as a young student and was influenced by his statement that ‘even the mediocre can have adventures and even the fearful can achieve’.

Sources:

Edmund Hillary, ‘Nothing Venture, Nothing Win’, The Travel Book Club, London, 1976.

Edward O. Wilson, Letters to a Young Scientist, Liveright Pub. Co., NY, 2013.