Tag Archives: experimental mechanics

Spatio-temporal damage maps for composite materials

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Earlier this year, my group published a new technique for illustrating the development of damage as a function of both space and time in materials during testing in a laboratory.  The information is presented in a damage-time map and shows where and when damage appears in the material.  The maps are based on the concept that damage represents a change in the structure of the material and, hence, produces changes in the load paths or stress distribution in the material.  We can use any of a number of optical techniques to measure strain, which is directly related to stress, across the surface of the material; and then look for changes in the strain distribution in real-time.  Wherever a permanent change is seen to occur there must also be permanent deformation or damage. We use image decomposition techniques that we developed some time ago [see ‘Recognizing strain‘ on October 28th, 2018], to identify the changes. Our damage-time maps remove the need for skilled operators to spend large amounts of time reviewing data and making subjective decisions.  They also allow a large amount of information to be presented in a single image which makes detailed comparisons with computer predictions easier and more readily quantifiable that, in turn, supports the validation of computational models [see ‘Model validation‘ on September 18th, 2012].

The structural integrity of composite materials is an on-going area of research because we only have a limited understanding of these materials.  It is easy to design structures using materials that have a uniform or homogeneous structure and mechanical properties which do not vary with orientation, i.e. isotropic properties.  For simple components, an engineer can predict the stresses and likely failure modes using the laws of physics, a pencil and paper plus perhaps a calculator.  However, when materials contain fibres embedded in a matrix, such as carbon-fibres in an epoxy resin, then the analysis of structural behaviour becomes much more difficult due to the interaction between the fibres and with the matrix.  Of course, these interactions are also what make these composite materials interesting because they allow less material to be used to achieve the same performance as homogeneous isotropic materials.  There are very many ways of arranging fibres in a matrix as well as many different types of fibres and matrix; and, engineers do not understand most of their interactions nor the mechanisms that lead to failure.

The image shows, on the left, the maximum principal strain in a composite specimen loaded longitudinally in tension to just before failure; and, on the right, the corresponding damage-time map indicating when and where damage developing during the tension loading.

Source:

Christian WJR, Dvurecenska K, Amjad K, Pierce J, Przybyla C & Patterson EA, Real-time quantification of damage in structural materials during mechanical testing, Royal Society Open Science, 7:191407, 2020.

Salt increases nanoparticle diffusion

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About two and half years ago, I wrote about an article we had published on the motion of nanoparticles [see ‘Slow moving nanoparticles‘ on December 13th, 2017] in which we had shown that, for very small particles at low concentrations, the motion of a particle is independent of its size and does not flow the well-known Stokes-Einstein law.  Our article presented convincing evidence from experiments to support our conclusions but was light on explanation in terms of the mechanics.  At the end of last year, we published a short article in Scientific Reports, in which we demonstrated that the motion of nanoparticles at low concentrations is dependent on the interaction of van der Waals forces and electrostatic forces.  Van der Waals forces are short-range attractive forces between uncharged molecules due to interacting dipole moments, whereas the electrostatic forces are the repulsion of electric charges.  We changed both of these forces by using salt solutions of different concentration and observing the changes in nanoparticle behaviour.  Increasing the molarity increases the diffusion of the particles until the solution is saturated, as shown in the picture for 50 nanometre diameter gold particles (that’s about half the diameter of a coronavirus particle or one thousandth of the diameter of a human hair).  Our findings have implications for understanding the behaviour of nanoparticles dispersed in biological media, which typically contain salt in solution, because the concentration of salt ions in the medium affects nanoparticle diffusion that has been shown to influence cellular uptake and toxicity.

Sources:

Coglitore D, Edwardson SP, Macko P, Patterson EA, Whelan MP, Transition from fractional to classical Stokes-Einstein behaviour in simple fluids, Royal Society Open Science, 4:170507, 2017.

Giorgi F, Coglitore D, Curran JM, Gilliland D, Macko P, Whelan M, Worth A & Patterson EA, The influence of inter-particle forces on diffusion at the nanoscale, Scientific Reports, 9:12689, 2019.

When seeing nothing is a success

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In November I went to Zurich twice: once for the workshop that I wrote about last week [see ‘Fake facts and untrustworthy predictions’ on December 4th, 2019]; and, a second time for a progress meeting of the DIMES project [see ‘Finding DIMES’ on February 6th, 2019].  The progress meeting went well.  The project is on schedule and within budget. So, everyone is happy and you are wondering why I am writing about it.  It was what our team was doing around the progress meeting that was exciting.  A few months ago, Airbus delivered a section of an A320 wing to the labs of EMPA who are our project partner in Switzerland, and the team at EMPA has been rigging the wing section for a simple bending test so that we can use it to test the integrated measurement system which we are developing in the DIMES project [see ‘Joining the dots’ on July 10th, 2019].  Before and after the meeting, partners from EMPA, Dantec Dynamics GmbH, Strain Solutions Ltd and my group at the University of Liverpool were installing our prototype systems to monitor the condition of the wing when we apply bending loads to it.  There is some pre-existing damage in the wing that we hope will propagate during the test allowing us to track it with our prototype systems using visible and infra-red spectrum cameras as well as electrical and optical sensors.  The data that we collect during the test will allow us to develop our data processing algorithms and, if necessary, refine the system design.  The final stage of the DIMES project will involve installing a series of our systems in a complete wing undergoing a structural test in the new Airbus Wing Integration Centre (AWIC) in Filton, near Bristol in the UK.  The schedule is ambitious because we will need to install the sensors for our systems in the wing in the first quarter of next year, probably before we have finished all of the tests in EMPA.  However, the test in Bristol probably will not start until the middle of 2020, by which time we will have refined our algorithm for data processing and be ready for the deluge of data that we are likely to receive from the test at Airbus.  The difference between the two wing tests besides the level of maturity of our measurement system, is that no damage should be detected in the wing at Airbus whereas there will be detectable damage in the wing section in EMPA.  So, a positive result will be a success at EMPA but a negative result, i.e. no damage detected, will be a success at Airbus.

The DIMES project has received funding from the Clean Sky 2 Joint Undertaking under the European Union’s Horizon 2020 research and innovation programme under grant agreement No. 820951.

 

The opinions expressed in this blog post reflect only the author’s view and the Clean Sky 2 Joint Undertaking is not responsible for any use that may be made of the information it contains.

Same problems in a different language

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I spent a lot of time on trains last week.  I left Liverpool on Tuesday evening for Bristol and spent Wednesday at Airbus in Filton discussing the implementation of the technologies being developed in the EU Clean Sky 2 projects MOTIVATE and DIMES.  On Wednesday evening I travelled to Bracknell and on Thursday gave a seminar at Syngenta on model credibility in predictive toxicology before heading home to Liverpool.  But, on Friday I was on the train again, to Manchester this time, to listen to a group of my PhD students presenting their projects to their peers in our new Centre for Doctoral Training called Growing skills for Reliable Economic Energy from Nuclear, or GREEN.  The common thread, besides the train journeys, is the Fidelity And Credibility of Testing and Simulation (FACTS).  My research group is working on how we demonstrate the fidelity of predictions from models, how we establish trust in both predictions from computational models and measurements from experiments that are often also ‘models’ of the real world.  The issues are similar whether we are considering the structural performance of aircraft [as on Wednesday], the impact of agro-chemicals [as on Thursday], or the performance of fusion energy and the impact of a geological disposal site [as on Friday] (see ‘Hierarchical modelling in engineering and biology‘ on March 14th, 2018) .  The scientific and technical communities associated with each application talk a different language, in the sense that they use different technical jargon and acronyms; and they are surprised and interested to discover that similar problems are being tackled by communities that they rarely think about or encounter.