Tag Archives: cracks

Scattering electrons reveal dislocations in material structure

Figure 9 from Yang et al, 2012. Map of plastic strain around the crack tip (0, 0) based on the full width of half the maximum of the discrete Fourier transforms of BSE images, together with thermoelastic stress analysis data (white line) and estimates of the plastic zone size based on approaches of Dugdale's (green line) and Irwin's (blue line; dimensions in millimetres).

Figure 9 from Yang et al, 2012. Map of plastic strain around the crack tip (0, 0) based on the full width of half the maximum of the discrete Fourier transforms of BSE images, together with thermoelastic stress analysis data (white line) and estimates of the plastic zone size based on approaches of Dugdale’s (green line) and Irwin’s (blue line; dimensions in millimetres).

It is almost impossible to manufacture metal components that are flawless.  Every flaw or imperfection in a metallic component is a potential site for the initiation of a crack that could lead to the failure of the component [see ‘Alan Arnold Griffith’ on April 26th, 2017].  Hence, engineers are very interested in understanding the mechanisms of crack initiation and propagation so that these processes can be prevented or, at least, inhibited.  It is relatively easy to achieve these outcomes by not applying loads that would supply the energy to drive failure processes; however, the very purpose of a metal component is often to carry load and hence a compromise must be reached.  The deep understanding of crack initiation and propagation, required for an effective and safe compromise, needs detailed measurements of evolution of the crack and of its advancing front or tip [depending whether you are thinking in three- or two-dimensions].  When a metal is subjected to repeated cycles of loading, then a crack can grow incrementally with each load cycle; and in these conditions a small volume of material, just ahead of the crack and into which the crack is about to grow, has an important role in determining the rate of crack growth.  The sharp geometry of the crack tip causes localisation of the applied load in the material ahead of the crack thus raising the stress sufficiently high to cause permanent deformation in the material on the macroscale.  The region of permanent deformation is known as the crack tip plastic zone.  The permanent deformation induces disruptions in the regular packing of the metal atoms or crystal lattice, which are known as dislocations and continued cyclic loading causes the dislocations to move and congregate around the crack tip.  Ultimately, dislocations combine to form voids in the material and then voids coalesce to form the next extension of the crack.  In reality, it is an oversimplification to refer to a crack tip because there is a continuous transition from a definite crack to definitely no crack via a network of loosely connected voids, unconnected voids, aggregated dislocations almost forming a void, to a progressively more dispersed crowd of dislocations and finally virgin or undamaged material.  If you know where to look on a polished metal surface then you could probably see a crack about 1 mm in length and, with aid of an optical microscope, you could probably see the larger voids forming in the material ahead of the crack especially when a load is applied to open the crack.  However, dislocations are very small, of the order tens of nanometres in steel, and hence not visible in an optical microscope because they are smaller than the wavelength of light.  When dislocations congregate in the plastic zone ahead of the crack, they disturb the surface of the metal and causing a change its texture which can be detected in the pattern produced by electrons bouncing off the surface.  At Michigan State University about ten years ago, using backscattered electron (BSE) images produced in a scanning electron microscope (SEM), we demonstrated that the change in texture could be measured and quantified by evaluating the frequency content of the images using a discrete Fourier transform (DFT).  We collected 225 square images arranged in a chessboard pattern covering a 2.8 mm by 2.8 mm square around a 5 mm long crack in a titanium specimen which allowed us to map the plastic zone associated with the crack tip (figure 9 from Yang et al, 2012).  The length of the side of each image was 115 microns and 345 pixels so that we had 3 pixels per micron which was sufficient to resolve the texture changes in the metal surface due to dislocation density.  The images are from our paper published in the Proceedings of the Royal Society and the one below (figure 4 from Yang et al, 2012) shows four BSE images along the top at increasing distances from the crack tip moving from left to right.  The middle row shows the corresponding results from the discrete Fourier transform that illustrate the decreasing frequency content of the images moving from left to right, i.e. with distance from the crack.  The graphs in the bottom row show the profile through the centre of the DFTs.  The grain structure in the metal can be seen in the BSE images and looks like crazy paving on a garden path or patio.  Each grain has a particular and continuous crystal lattice orientation which causes the electrons to scatter differently from it compared to its neighbour.  We have used the technique to verify measurements of the extent of the crack tip plastic zone made using thermoelastic stress analysis (TSA) and then used TSA to study ‘Crack tip plasticity in reactor steels’ [see post on March 13th, 2019].

Figure 4 from Yang et al, 2012. (a) Backscattered electron images at increasing distance from crack from left to right; (b) their corresponding discrete Fourier transforms (DFTs) and (c) a horizontal line profile across the centre of each DFT.

Figure 4 from Yang et al, 2012. (a) Backscattered electron images at increasing distance from crack from left to right; (b) their corresponding discrete Fourier transforms (DFTs) and (c) a horizontal line profile across the centre of each DFT.

Reference: Yang, Y., Crimp, M., Tomlinson, R.A., Patterson, E.A., 2012, Quantitative measurement of plastic strain field at a fatigue crack tip, Proc. R. Soc. A., 468(2144):2399-2415.

Condition-monitoring using infrared imaging

If you have travelled in Asia then you will probably have experienced having your health monitored by infrared cameras as you disembarked from your flight.  It has been common practice in many Asian countries since long before the COVID-19 pandemic and perhaps will become more usual elsewhere as a means of easily identifying people with symptoms of a fever that raises their body temperature.  Since, research has shown that infrared thermometers are slightly more responsive as well as quicker and easier to use than other types of skin surface thermometers [1].  In my research group, we have been using infrared cameras for many years to monitor the condition of engineering structures by evaluating the distribution of load or stress in them [see ‘Counting photons to measure stress‘ on November 18th, 2015 and  ‘Insidious damage‘ on December 2nd, 2015].  In the DIMES project, we have implemented a low-cost sensor system that integrates infrared and visible images with information about applied loads from point sensors, which allows the identification of initiation and tracking of damage in aircraft structures [2].  I reported in December 2019 [see ‘When seeing nothing is a success‘] that we were installing prototype systems in a test-bench at Empa.  Although the restrictions imposed by the pandemic have halted our tests, we were lucky to obtain data from our sensors during the propagation of damage in the section of wing at Empa before lockdown.  This is a landmark in our project and now we are preparing to install our system in test structures at Airbus once the pandemic restrictions are relaxed sufficiently.  Of course, we will also be able to use our system to monitor the health of the personnel involved in the test (see the top image of one of my research team) as well as the health of the structure being tested – the hardware is the same, it’s just the data processing that is different.

The image is a composite showing images from a visible camera (left) and processed data from infrared camera overlaid on the same visible image (right) from inside a wing box during a test at Empa with a crack extending from left to right with its tip surrounded by the red area in the right image.  Each nut in the image is about 20 mm in diameter and a constant amplitude load at 1.25 Hz was being applied causing a wing tip displacement of 80 mm +/- 15 mm.

The University of Liverpool is the coordinator of the DIMES project and the other partners are Empa, Dantec Dynamics GmbH and Strain Solutions Ltd.

The DIMES project has received funding from the Clean Sky 2 Joint Undertaking under the European Union’s Horizon 2020 research and innovation programme under grant agreement No. 820951.

 

The opinions expressed in this blog post reflect only the author’s view and the Clean Sky 2 Joint Undertaking is not responsible for any use that may be made of the information it contains.

References

[1] Burnham, R.S., McKinley, R.S. and Vincent, D.D., 2006. Three types of skin-surface thermometers: a comparison of reliability, validity, and responsiveness. American journal of physical medicine & rehabilitation, 85(7), pp.553-558.

[2] Middleton, C.A., Gaio, A., Greene, R.J. and Patterson, E.A., 2019. Towards automated tracking of initiation and propagation of cracks in aluminium alloy coupons using thermoelastic stress analysis. Journal of Nondestructive Evaluation, 38(1), p.18.

Crack tip plasticity in reactor steels

Amplitude of temperature in steel due to a cyclic load with a crack growing from left to right along the horizontal centre line with the stress concentration at its tip exhibiting the peak values. The wedge shapes in the left corners are part of the system.

At this time of year the flow into my inbox is augmented daily by prospective PhD students sending me long emails describing how their skills, qualifications and interests perfectly match the needs of my research group, or sometimes someone else’s group if they have not been careful in setting up their mass mailing.  At the moment, I have four PhD projects for which I am looking for outstanding students; so, because it will help prospective students and might interest my other readers but also because I am short of ideas for the blog, I plan to describe one project per week for the next month.

The first project is about the effect of hydrogen on crack tip plasticity in reactor steels.  Fatigue cracks grow in steels by coalescing imperfections in the microstructure of the material until small voids are formed in areas of high stress.  When these voids connect together a crack is formed.  Repeated loading and unloading of the material provides the energy to move the imperfections, known as dislocations, and geometric features in structures are stress concentrators which focus this energy causing cracks to be formed in their vicinity.  The movement of dislocations causes permanent, or plastic deformation of the material.  The sharp geometry of a crack tip becomes a stress concentrator creating a plastic zone in which dislocations pile up and voids form allowing the crack to extend [see post on ‘Alan Arnold Griffith‘ on April 26th, 2017].  It is possible to detect the thermal energy released during plastic deformation using a technique known as thermoelastic stress analysis [see ‘Counting photons to measure stress‘ on November 18th 2015] as well as to measure the stress field associated with the propagating crack [1].  One of my current PhD students has been using this technique to investigate the effect of irradiation damage on the growth of cracks in stainless steel used in nuclear reactors.  We use an ion accelerator at the Dalton Cumbrian Facility to introduce radiation damage into specimens the size of a postage stamp and afterwards apply cyclic loads and watch the fatigue crack grow using our sensitive infra-red cameras.  We have found that the irradiation reduced the rate of crack growth and we will be publishing a paper on it shortly [and a PhD thesis].  In the new project, our industrial sponsors want us to explore the effect of hydrogen on crack growth in irradiated steel, because the presence of hydrogen is known to accelerate fatigue crack growth [2] which is believe to happen as a result of hydrogen atoms disrupting the formation of dislocations at the microscale and localising plasticity at crack tip on the mesoscale.  However, these ideas have not been demonstrated in experiments, so we plan to do this using thermoelastic stress analysis and to investigate the combined influence of hydrogen and irradiation by developing a process for pre-charging the steel specimens with hydrogen using an electrolytic cell and irradiating them using the ion accelerator.  Both hydrogen and radiation are present in a nuclear reactor and hence the results will be relevant to predicting the safe working life of nuclear reactors.

The PhD project is fully-funded for UK and EU citizens as part of a Centre for Doctoral Training and will involve a year of specialist training followed by three years of research.  For more information following this link.

References:

  1. Yang, Y., Crimp, M., Tomlinson, R.A., Patterson, E.A., 2012, Quantitative measurement of plastic strain field at a fatigue crack tip, Proc. R. Soc. A., 468(2144):2399-2415.
  2. Matsunaga, H., Takakuwa, O., Yamabe, J., & Matsuoka, S., 2017, Hydrogen-enhanced fatigue crack growth in steels and its frequency dependence. Phil. Trans. R. Soc. A, 375(2098), 20160412

Finding DIMES

A couple of weeks ago I wrote about the ‘INSTRUCTIVE final reckoning’ (see post on January 9th).  INSTRUCTIVE was an EU project, which ended on December 31st, 2018  in which we demonstrated that infra-red cameras could be used to monitor the initiation and propagation of cracks in aircraft structures (see Middleton et al, 2019).  Now, we have seamlessly moved on to a new EU project, called DIMES (Development of Integrated MEasurement Systems), which started on January 1st, 2019.  To quote our EU documentation, the overall aim of DIMES is ‘to develop and demonstrate an automated measurement system that integrates a range of measurement approaches to enable damage and cracks to be detected and monitored as they originate at multi-material interfaces in an aircraft assembly’.  In simpler terms, we are going to take the results from the INSTRUCTIVE project, integrate them with other existing technologies for monitoring the structural health of an aircraft, and produce a system that can be installed in an aircraft fuselage and will provide early warning on the formation of cracks.  We have two years to achieve this target and demonstrate the system in a ground-based test on a real fuselage at an Airbus facility.  This was a scary prospect until we had our kick-off meeting and a follow-up brainstorming session a couple of weeks ago.  Now, it’s a little less scary.  If I have scared you with the prospect of cracks in aircraft, then do not be alarmed; we have been flying aircraft with cracks in them for years.  It is impossible to build an aircraft without cracks appearing, possibly during manufacturing and certainly in service – perfection (i.e. cracklessness) is unattainable and instead the stresses are maintained low enough to ensure undetected cracks will not grow (see ‘Alan Arnold Griffith’ on April 26th, 2017) and that detected ones are repaired before they propagate significantly (see ‘Aircraft inspection’ on October 10th, 2018).

I should explain that the ‘we’ above is the University of Liverpool and Strain Solutions Limited, who were the partners in INSTRUCTIVE, plus EMPA, the Swiss National Materials Laboratory, and Dantec Dynamics GmbH, a producer of scientific instruments in Ulm, Germany.  I am already working with these latter two organisations in the EU project MOTIVATE; so, we are a close-knit team who know and trust each other  – that’s one of the keys to successful collaborations tackling ambitious challenges with game-changing outcomes.

So how might the outcomes of DIMES be game-changing?  Well, at the moment, aircraft are designed using computer models that are comprehensively validated using measurement data from a large number of expensive experiments.  The MOTIVATE project is about reducing the number of experiments and increasing the quality and quantity of information gained from each experiment, i.e. ‘Getting Smarter’ (see post on June 21st 2017).  However, if the measurement system developed in DIMES allowed us to monitor in-flight strain fields in critical locations on-board an aircraft, then we would have high quality data to support future design work, which would allow further reductions in the campaign of experiments required to support new designs; and we would have continuous comprehensive monitoring of the structural integrity of every aircraft in the fleet, which would allow more efficient planning of maintenance as well as increased safety margins, or reductions in structural weight while maintaining safety margins.  This would be a significant step towards digital twins of aircraft (see ‘Fourth industrial revolution’ on July 4th, 2018 and ‘Can you trust your digital twin?’ on November 23rd, 2016).

The INSTRUCTIVE, MOTIVATE and DIMES projects have received funding from the Clean Sky 2 Joint Undertaking under the European Union’s Horizon 2020 research and innovation programme under grant agreements No. 685777, No. 754660 and No. 820951 respectively.

The opinions expressed in this blog post reflect only the author’s view and the Clean Sky 2 Joint Undertaking is not responsible for any use that may be made of the information it contains.

Sources:

Middleton CA, Gaio A, Greene RJ & Patterson EA, Towards automated tracking of initiation and propagation of cracks in Aluminium alloy coupons using thermoelastic stress analysis, J. Non-destructive Testing, 38:18, 2019